Prediksi masa simpan emulsi virgin coconut oil-sari jeruk berdasarkan perubahan bilangan peroksida menggunakan metode accelerated shelf-life testing

Authors

  • Zakir Sabara Jurusan Teknik Kimia, Fakultas Teknologi Industri, Universitas Muslim Indonesia
  • Lastri Wiyani Jurusan Teknik Kimia, Fakultas Teknologi Industri, Universitas Muslim Indonesia
  • G Gusnawati Jurusan Teknik Kimia, Fakultas Teknologi Industri, Universitas Muslim Indonesia
  • Andi Aladin Jurusan Teknik Kimia, Fakultas Teknologi Industri, Universitas Muslim Indonesia
  • Vita Febrianti Mansyu Jurusan Teknik Kimia, Fakultas Teknologi Industri, Universitas Muslim Indonesia
  • Chusnul Azzahrah Jurusan Teknik Kimia, Fakultas Teknologi Industri, Universitas Muslim Indonesia

DOI:

https://doi.org/10.35891/gnfgw390

Keywords:

emulsion, virgin coconut oil, orange juice, self-life, peroxide number

Abstract

Virgin Coconut Oil–Orange Juice Emulsion (EVCO-SJ) is formulated by mixing Virgin Coconut Oil with Orange Juice and other additives. EVCO-SJ was developed as an alternative form of VCO consumption to reduce the oily sensation in the mouth when consuming VCO directly. Determining the product's shelf life is a crucial aspect because it is closely related to determining the expiration date of food products. This study aims to predict the shelf life of EVCO-SJ based on changes in peroxide value using the Accelerated Shelf-Life Testing (ASLT) method. EVCO-SJ is made by mixing VCO and orange juice (8:2) using gum arabic (0.75%) as emulsifier and homogenized using a Tokebi device at 23,000 rpm for 2 minutes. EVCO-SJ is stored at three temperature variations, namely 30 °C, 45 °C, and 55 °C, with storage time intervals of 0, 7, 14, 21, 28, and 35 days. The observed quality parameter is the peroxide value as an early indicator of lipid oxidation. Data on changes in peroxide value are analyzed using the Arrhenius model in the ASLT method to predict shelf life. The results showed that increasing storage temperature accelerated the rate of lipid oxidation in EVCO-SJ, as indicated by an increase in the peroxide value during storage. Predicted shelf life of EVCO-SJ based on the ASLT method indicated that the shelf life at 30°C, 45°C, and 55°C was 146.34 days, 83.46 days, and 59.06 days, respectively. These results provide scientific information regarding the oxidative stability of EVCO-SJ and can serve as a basis for determining shelf life and developing VCO-based emulsion products with measurable quality and shelf life.

 

References

Ardyanti, D. K., Yuwono, S. S., & Septifani, R. (2024). Pendugaan umur simpan kukis kecambah kedelai terelisitasi dengan metode Accelerated Shelf Life Testing model Arrhenius. Jurnal Pangan dan Agroindustri, 12(3), 165–174. https://doi.org/10.21776/ub.jpa.2024.012.03.5

Calligaris, S., Lucci, P., Milani, A., Rovellini, P., Lagazio, C., & Conte, L. (2022). Application of accelerated shelf-life test (ASLT) procedure for the estimation of the shelf-life of extra virgin olive oils: A validation study. Food Packaging and Shelf Life, 33, 100990. https://doi.org/10.1016/j.fpsl.2022.100990

Fitriani, N., Aladin, A., & Kalsum, U. (2025). Laju penurunan kualitas virgin coconut oil (VCO) dalam wadah botol kaca bening dengan metode Accelerated Shelf Life Testing (ASLT). JUTIN: Jurnal Teknik Industri Terintegrasi, 8(1), 1151–1160.

Gajendiran, V., Alkathiri, D. S. M. S., Jashaool, A. A. S., Alkathiri, H. B. S., & Chellakannu, M. (2025). Optimizing virgin coconut oil production: A comparative study of extraction methods and quality parameters. International Journal of Engineering Research and Development, 21(6), 93–97. https://ijerd.com/paper/vol21-issue6/21069397.pdf

Gan, J., Zhao, M., He, Z., Sun, L., Li, X., & Feng, Y. (2022). The effects of antioxidants and packaging methods on inhibiting lipid oxidation in deep fried crickets (Gryllus bimaculatus) during storage. Foods, 11(3), 326. https://doi.org/10.3390/foods11030326

Ghani, N. A. A., Channip, A. A., Hwa, P. C. H., Ja’afar, F., & Yasin, H. M. (2018). Physicochemical properties, antioxidant capacities, and metal contents of virgin coconut oil produced by wet and dry processes. Food Science and Nutrition, 6, 1298–1306. https://doi.org/10.1002/fsn3.671

Ghelichi, S., Hajfathalian, M., Yesiltas, B., Sørensen, A. D. M., García-Moreno, P. J., & Jacobsen, C. (2023). Oxidation and oxidative stability in emulsions. Comprehensive Reviews in Food Science and Food Safety, 22(3), 1864–1911.

Hennebelle, M., Villeneuve, P., Durand, E., Lecomte, J., & van Duynhoven, J. P. M. (2024). Lipid oxidation in emulsions: New insights from the past two decades. Progress in Lipid Research, 95, 101275. https://doi.org/10.1016/j.plipres.2024.101275

Malingkas, T. D., Tongkeles, N. S., Manesi, D., Fadillah, R., Lele, O. K., Martini, D. K. T., & Banamtuan, E. (2023). VCO rancidity analysis refers to fermentation time that produced by gradual heating method. International Journal of Advanced Engineering Research and Science, 10(4), 63–67. https://doi.org/10.22161/ijaers.104.7

Merrx, D. W. H., Swager, A., van Velzen, E. J. J., van Duynhoven, J. P. M., & Hennebelle, M. (2021). Quantitative and predictive modelling of lipid oxidation in food emulsions. Antioxidants, 10(2), 287. https://doi.org/10.3390/antiox10020287

Nguyen, K. A., Hennebelle, M., van Duynhoven, J. P. M., Dubbelboer, A., Boerkamp, V. J. P., & Wierenga, P. A. (2023). Mechanistic kinetic modelling of lipid oxidation in vegetable oils to estimate shelf-life. Food Chemistry, 433, 137266. https://doi.org/10.1016/j.foodchem.2023.137266

Nuraini, V. dan Widanti, Y. A. 2020. Pendugaan Umur Simpan Makanan Tradisional Berbahan Dasar Beras dengan Metode Accelerated Shelf-Life Testing (ASLT) Melalui Pendekatan Arrhenius dan Kadar Air Kritis. Jurnal Agroteknologi, Vol. 14 No. 02: 189.

Nurhasanah, S., Setyadi, A., Munarso, S. J., Subroto, E. dan Filianty, F. 2022. Shelf-Life Prediction of Peanut Oil (Arachis hypogaea L.) Using an Accelerated Shelf-Life Testing (ASLT) Method in the Polypropylene Packaging. IOP Conference Series: Earth and Environmental Science, Vol. 1024 No. 1 : 1–12.

Pagey, S. V., Landge, B. P., & Nakhale, S. (2025). Lipid oxidation in food systems: Mechanisms, detection methods, and prevention strategies. International Journal of Applied Research, 11(5), 82–88.

Prasanna, N. S., Selvakumar, M., Choudhary, N., & Raghavarao, K. S. M. S. (2024). Virgin coconut oil: Wet production methods and food applications – A review. Sustainable Food Technology, 5(2), 1391–1408. https://doi.org/10.1039/D4FB00093E

Puspitasari, E., Sutan, S.M., dan Lastriyanto, A. 2020. Pendugaan umur simpan Kripik Kelapa (Cocos nucifera) Menggunakan Metode Accelerated Shelf-Life Testing (ASLT) Model pendekatan Persamaan Arrhenius. Journal Keteknikan Pertanian Tropis dan Biosistem 8(1): 36-45.

Saragih, M. H., Silaban, S., & Eddiyanto. (2023). The impact of temperature and antioxidants on oxidation and the formation of trans fatty acids in several palm oil derivatives. Al Kimiya: Jurnal Ilmu Kimia dan Terapan, 10(2), 74–86. http://dx.doi.org/10.15575/ak.v10i2.25256

Suhag, R., Kellil, A., Ferrentino, G., Morozova, K., Zatelli, D., & Scampicchio, M. (2024). Lipid oxidation kinetics and antioxidant efficiency in foods using isothermal calorimetry. Trends in Food Science & Technology, 145, 104801. https://doi.org/10.1016/j.tifs.2024.104801

Wang, D., Xiao, H., Lyu, X., Chen, H., & Wei, F. (2023). Lipid oxidation in food science and nutritional health: A comprehensive review. Oil Crop Science, 8(1), 35–44. https://doi.org/10.1016/j.ocsci.2023.02.002

Wiyani, L., Aladin, A. Yani, S. dan Rahmawati. 2016. “Stability of Virgin Coconut Oil Emulsion with mixed Emulsifiers Tween 80 and Span 80. ARPN Journal of Engineering and Applied Sciences. Vol 11. No.8, hal.5198-5202

Wiyani, L., Aladin, A., Yani, S., Muthmainnah, S., & Mandang, H.,2018. Effect Of Sucrose and Citric Acid Addition in the Virgin Coconut Oil Emulsion. IOP Conference Series: Earth and Environmental Science Vol 175.: 1315.

Wiyani, L., Aladin, A., Rahmawati, & Mustafiah. (2020a). Characteristics of virgin coconut oil with honey and citric acid. Advances in Engineering Research, 194, 246–250. https://doi.org/10.2991/aer.k.200325.048

Wiyani, L., Aladin, A., Sabara, Z., Mustafiah, & Rahmawati. (2020b). Pengaruh waktu dan kecepatan homogenisasi terhadap emulsi virgin coconut oil–sari jeruk dengan emulsifier gum arab. Journal of Chemical Process Engineering, 5(2), 50–55. https://jurnal.fti.umi.ac.id/index.php/JCPE/article/view/903

Wiyani, L., Aladin, A., Rahmawati, & Mustafiah. (2021). The physical and chemical properties of VCO emulsion with citrus extract. IOP Conference Series: Earth and Environmental Science, 712(1), 012046. https://doi.org/10.1088/1755-1315/712/1/012046

Zeng, Y.-Q., He, J.-T., Hu, B.-Y., Li, W., Deng, J., Lin, Q.-L., & Fang, Y. (2024). Virgin coconut oil: A comprehensive review of antioxidant activity and mechanisms contributed by phenolic compounds. Critical Reviews in Food Science and Nutrition, 64(4), 1052–1075. https://doi.org/10.1080/10408398.2022.2113361

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Published

2026-03-25

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